Freeze Concentration, sometimes mistakenly called Freeze Distillation is a way to increase the ABV of wine or beer to that of a spirit. It's quite capable of increasing to a 50% + by multiple concentrations.
The method is simple.
Fill a 2 litre bottle with some old wine of say 12% and put it into a freezer for about 3 days, leave the lid loose so it can be removed easier.
Remove the bottle, remove the lid and place it upside down in a 1 litre glass jug.
As water freezes at zero C and alcohol freezes at -114 C, the alcohol will start to drip into the jug leaving behind the water in ice form.
You will notice that the ice in the bottle will begin to lose it's colour. Once you have collected approx 1 litre, the ice in the bottle will have gone almost clear as some alcohol will still be present.
In 2 litres of 12% wine there is 1.760 litres of water, so in theory, if you remove 880 ml of water in the form of ice you are left with 1.120 litres of 24% spirit with intense flavour as doing this concentrates flavour as well, it also makes the product clearer by leaving any particles suspended in the ice.
There is no simple way to measure this as it contains other elements such as sugars etc, so a spirit hydrometer cannot be used, and as of yet I cannot find a calculator on the web.
Some may say "What about the Acetone, Methanol and Acetates than are normally removed by distillation, surely they are still there doing the freeze method".
One brewery in Scotland said "We use this method in our very high ABV beers and have full UK approval for our products.The unwanted alcohols are in such small quantities because we do not ferment the wort over 12%. Shop bought wines & beers contain the same unwanted alcohols but you don't hear people complaining about it, also freeze concentration is legal in the UK, so no distilling license was required by us".
Those of us who make or buy Vodka and wish to increase the ABV for special blends can do this the same way, and can measure the finished product with a spirit hydrometer when it's brought back up to 20C.
It can also be done with beer as BrewDog have proved, and with cider to make Applejack.
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